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- Weigh 1.852 g NH4F and add it to 100 mL of water. Add 20.50 g (22.78 mL) ammonium hydroxide solution. Store this in a bottle so you can reuse it later. This is the “ammonium fluoride/ammonium hydroxide stock solution”. If you already have stock solution prepared you can skip down to step 2.
- Mix 4.7 g (5.0 mL) TEOS and 8.68 g (11.0 mL) ethanol in a beaker. This is the “alkoxide solution”.
- Mix 7.0 g (7.0 mL) water and 8.68 g (11.0 mL) ethanol in another beaker. Add 0.364 g (0.371 mL, ~8-10 drops from a disposable pipette) of ammonium fluoride/ammonium hydroxide stock solution. This mixture is the “catalyst solution”.
- Pour the catalyst solution into the alkoxide solution and stir. This is the “sol”.
- Pour the sol into molds and allow gel to form. Gel time is approximately 8-15 min.
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